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Atmospheric Pressure Ionization Test Solution [700000889]

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Atmospheric Pressure Ionization Test Solution [700000889]

The Atmospheric Pressure Ionization Test Solution kit is intended for system performance verification of ZMD, QTof I/II/APIUS/Micro, PlatformII, QuattroII, LCT. This kit is designed for use by a Waters certified engineer or user as part of a performance maintenance or qualification activity.  Protocols in the use of this kit are available via the purchase of Waters qualification services or self directed qualification training and license.  

The Atmospheric Pressure Ionization Test Solution kit contains:

  • Set Up Solution: 2 ng/μL reserpine, 25 ng/μL PPG 1000, 50 ng/μL triacetyl-B-cyclodextrin in 50/50 acetonitrile/4 mM ammonium acetate, 10 mL .

 

This solution is used with quadrupole MS's to perform mass scale and resolution setup check. Note that many of the compounds are concentrated and should be diluted for use with the Xevo® Series, or even the SQD.

  • Calibration Solution: 2 μg/μL sodium iodide, 50 ng/μL cesium iodide, in 50/50 2-propanol/water, 10 mL.

 

One of the most commonly used solutions for Waters MS's and is used to calibrate the majority of single and triple quadrupole instruments. API calibration solution is run to verify mass to charge (m/z) ratio accuracy. It is infused into the MS and the instrument's calibrations are run across a pre-selected mass range. Calibrations are performed in static, scanning, and scan speed compensation modes. A spectrum is acquired and the calibrated mass positions are checked to ensure they are within predefined limits. This solution can be used to calibrate both MS1 and MS2 on a triple quad. (700001593)

  • Horse Heart Myoglobin: 3.4 mg horse heart myoglobin solid in 4 mL amber screw top vial.

 

Used as a calibration standard or can be used for ESI positive sensitivity testing. (similar to: 700004749)

  • Raffinose: 5 ng/μL raffinose in 50/50 acetonitrile/water, 10 mL.

 

Used to perform sensitivity testing in ESI negative mode (older detectors such as the Quattro Micro).

  • Reserpine Stock Solution: 50 ng/μL reserpine stock solution in 50/50 methanol/water, 10 mL.

 

Used to optimize tune parameters and signal and the working solution is used to perform ESI positive sensitivity testing. (similar to 700001673)

  • Reserpine Working Solution: 1 pg/μL reserpine working solution in 50/50 methanol/water, 10 mL.

 

Used to optimize tune parameters and signal and the working solution is used to perform ESI positive sensitivity testing. (see: 700001673)

  • p-nitrophenol Stock: 50 ng/μL p-nitrophenol stock solution in 50/50 methanol/water, 10 mL.

 

Used to optimize tune parameters and the working solution is used to perform APCI/ESCI sensitivity testing in negative mode.

  • p-nitrophenol Working Solutions: 2 pg/μL p-nitrophenol working solution in 50/50 methanol/water, 10 mL.

Used to optimize tune parameters and the working solution is used to perform APCI/ESCI sensitivity testing in negative mode.

 

Store at room temperature.

System Performance Standards Key

Set Up

Setup standards are used upon installation of a new system, start-up of a system which has been idle for a period of time, or to re-start a system that has been moved to a new location. These standards may include multiple components within a kit which allow step by step setup and calibration, or they can be single mixtures which will enable a full system assessment and initialization.

Calibration

These standards can be used for instrument calibration. Calibration is usually performed at a frequency that minimizes the risk of being out of calibration, in addition to major events suc h as when the instrument is moved and upon any major repair. Calibration can be confirmed as often as your standard operating procedures recommend. Look for solutions to calibrate your MS mass accuracy and resolution, UV detector linearity, UV and Fluorescence detector wavelength accuracy, injector accuracy and precision, and solvent system flow rate accuracy.

Performance

Your system is comprised of many interdependent components working together. An issue with any one component can produce erroneous final results. All components performing correctly will produce results within an expected variability. Some of the system components include mobile phase, column, tubing, pumping, injecting, temperature controlling, detecting, data collection rate, and integration
parameters. An issue in any one of the components listed can affect your result.
 
Performance Check Standards should be utilized on a routine basis. This includes anytime a column is changed, a method is changed, the instrument is moved, or confirmation of system performance is desired. Confirming the performance of your system can be done on a system basis with suitability standards or per individual instrument component. Benchmark performance should be established after
calibration and confirmed regularly.

Tuning

These Mass Spectrometry solutions are used routinely and are available for every ionization mode. Use the solution to optimize the mass spectrometer setting for optimal signal either manually or through Intellistart.

Hazardous

This product contains hazardous material which requires special freight handling. Additional charges may apply.

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